Nanostructuring of surfaces of metalloceramic and ceramic materials by electron-beams

• DOI: 10.1007/s11182-008-9073-7
• Publication Date: 2008-10-16T08:50:49Z
• Authors: N. N. Koval’; Yu. F. Ivanov
• Keywords: Nanocrystalline material; Acceleration voltage; Pulse duration

An electron-emitting source generating a low-energy beam measuring 1–3 cm in diameter, with current up to 300 A, pulse duration within 50–200 µs, and pulse repetition frequency up to 10 Hz is investigated in a gas-filled diode with a mesh plasma cathode at the accelerating voltage up to 25 kV. The beam is transported in a longitudinal pulsed magnetic field to a distance of up to 30 cm towards the region of its interaction with a solid. For the current densities up to 100 A/cm2, it provides the power density as high as 10–100 J/cm2 sufficient to melt surfaces of metals, alloys, and composite (metalloceramic) materials within one or a few pulses. This makes this beam useful for modification of material surfaces and articles made thereof. Using the methods of optical, scanning and diffraction electron microscopy, by building micro-and nanohardness profiles, and via identification of the treated surface roughness, the phase composition and the substructure state of the materials subjected to pulsed low-energy e-beam of sub-millimeter durations are investigated. Formation of submicro-and nanocrystalline multi-phase structure is observed, which ensures a multiple increase in physico-mechanical and tribological characteristics of the treated material.