Experimental characterization and strengthening mechanism of process-structure-property of selective laser melted 316 L

• DOI: 10.1016/j.matchar.2023.112753
• Publication Date: 2023-02-23T03:56:09Z
• Authors: Yefeng Chen; Xiaowei Wang; Dong Li; Dewen Zhou; Yong Jiang; Xinyu Yang; Chenglu Liu; Sean B. Leen; Jianming Gong
• Keywords: Selective laser melting; 0205 materials engineering; 316 L; Tensile property; 02 engineering and technology; 0210 nano-technology; Heat treatment; Microstructure

Heat treatment is the most common method to relieve residual stress and to adjust tensile properties in additively manufactured material. However, the well-known strengthening factors (e.g., dislocation density, cellular sub-structure, low angle grain boundaries, nano-oxide particle) in selective laser melted 316 L (SLM 316 L) are strongly influenced by heat-treatment temperature. In this work, horizontal and vertical oriented SLM 316 L specimens are heat treated from 550 °C to 1150 °C, followed by tensile tests and microstructural characterization. With increasing temperature, strength (e.g., yield strength, ultimate tensile strength) is found to decrease and elongation is found to increase. The heat treatments of 550 °C, 650 °C and 750 °C lead to coarsening of cellular sub-structure. Furthermore, the cellular sub-structure and melt boundaries annihilate at 950 °C. When the temperature reaches 1150 °C, SLM 316 L has finished recrystallization with volume fraction of nano-oxide particles increasing greatly. Based on microstructural characterization, the proposed relationship, considering strengthening mechanisms of cellular sub-structure, nano-oxide particle and grain boundaries, give satisfactory accuracy to predict yield strength for horizontal orientation. The yield strength for vertical orientation can also be predicted by this relationship when modified by consideration of anisotropy of columnar grains and lack-of-fusion defects. The anisotropy and lack-of-fusion lead to 5.4% reduction in yield strength for the vertical orientation. This work establishes quantitative relationships for heat treatment-microstructure-property, in which the anisotropy of tensile properties is considered.