Synthesis and Characterization of Ordered and Disordered Mesoporous Alumina as High-Performance Molybdenum-99 Adsorbents

Characterization
DOI: 10.17146/aij.2021.1000 Publication Date: 2021-04-26T13:58:43Z
ABSTRACT
Normal 0 false EN-US X-NONE /* Style Definitions */ table.MsoNormalTable {mso-style-name:"Table Normal"; mso-tstyle-rowband-size:0; mso-tstyle-colband-size:0; mso-style-noshow:yes; mso-style-priority:99; mso-style-parent:""; mso-padding-alt:0cm 5.4pt 0cm 5.4pt; mso-para-margin:0cm; mso-para-margin-bottom:.0001pt; mso-pagination:widow-orphan; font-size:10.0pt; font-family:"Times New Roman","serif";} Molybdenum-99 ( 99 Mo) is the parent radioisotope of technetium-99m 99m Tc) , an essential medical for diagnostic agents in nuclear medicine. In Mo/ Tc generator, a chromatography column system with Mo adsorbent as filler usually used to produce hospitals. However, it still challenging find high-performance adsorbents adsorption . We have synthesized both ordered and disordered mesoporous alumina compared their performance s These materials were prepared via soft-templated method using triblock copolymer template followed by air calcin ation at 400 ° C. T he amount nitric acid (HNO 3 ) drying time adjusted systematically synthesize alumina. The obtained characterized low-and wide-angle X -ray diffractions (XRD) nitrogen adsorption-desorption, ther mo gravimetric analysis (TGA), scanning electron microscop y (SEM), transmission (TEM). capacit ies these evaluated batch method. experimental results show that has higher capacity 72.06 mg (Mo) g -1 than 50.12 indicate excellent potential o rdered generator
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