Alkoxyalkanol Modified Ti(OCHMe<sub>2</sub>)<sub>4</sub>: Synthesis and Characterization of Novel [(OPr<sup>i</sup>)<sub>4-n</sub>Ti (OC<sub>2</sub>H<sub>4</sub>OR)<sub>n</sub>]
Stoichiometry
DOI:
10.4028/www.scientific.net/amr.584.415
Publication Date:
2012-10-26T09:45:44Z
AUTHORS (7)
ABSTRACT
Novel structural arrangements for alkoxyalkanol modified titanium tetraisopropoxide [(Ti(OPr i ) 4 , TPT] were obtained from stoichiometric reactions between TPT and alkoxyalkanols {HOCH 2 CH OR,where R= Me, Et}. All the 1:1, 1:2, 1:3 1:4 in refluxing benzene form mononuclear species [(OPr 4-n Ti(OC H OR) n ]. these compounds can be purified by distillation under reduced pressure. On basis of IR NMR ( 1 & 13 C) spectral studies all derivatives have been tetrahedral geometry around atom.
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