Development of Wet Environmental TEM (Wet-ETEM) for In Situ Studies of Liquid-Catalyst Reactions on the Nanoscale
Titanium
Polymers
Cobalt
02 engineering and technology
Diamines
01 natural sciences
Catalysis
Phase Transition
Ruthenium
0104 chemical sciences
Microscopy, Electron
Nylons
Nitriles
Nanotechnology
0210 nano-technology
DOI:
10.1017/s143192760201005x
Publication Date:
2003-10-15T16:19:08Z
AUTHORS (1)
ABSTRACT
We present the development of in situ wet environmental
transmission electron microscopy (Wet-ETEM) for direct probing
of controlled liquid–catalyst reactions at operating
temperatures on the nanoscale. The first nanoscale imaging and
electron diffraction of dynamic liquid hydrogenation and
polymerization reactions in the manufacture of polyamides reported
here opens up new opportunities for high resolution studies
of a wide range of solution–solid and
solution–gas–solid reactions in the chemical and
biological sciences.
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