Development of two-stage multi-anvil apparatus for low-temperature measurements

• DOI: 10.4279/pip.110006
• Publication Date: 2019-08-12T17:05:26Z
• Authors: K. Ishigaki; J. Gouchi; S. Nagasaki; J. G. Cheng; Y. Uwatoko
• Keywords: High pressure; Science; Physics; QC1-999; Q; 0103 physical sciences; low temperature; High pressure, low temperature, multi anvil; 01 natural sciences; multi anvil

The two-stage 6-8 multi-anvil (MA8) apparatus is an important large-volume, high-pressure technique that has been widely used in the high pressure mineralogy and material synthesis, mainly at room temperature or above. Recently, we have successfully developed a two-stage MA8 apparatus for low-temperature physical property measurements. The first-stage anvils at top and bottom sides are fabricated as a single piece in order to reduce the total size of the cylindrical module, which is put in a top-loading high pressure cryostat and compressed by a 1000 ton hydraulic press. A castable, split octahedral gasket with integrated fin was specifically designed in order to introduce the electrical leads from the inside sample container filled with a liquid pressure transmitting medium. By using tungsten carbide (WC) second-stage cubes with a truncated edge length of 3 mm and an octahedral gasket with an edge length of 6 mm, we have successfully generated pressure over 20 GPa at room temperature. Since the high pressure limit can be pushed to nearly 100 GPa by using the sintered diamond second-stage cubes, our MA8 apparatus has a great potential to expand the current pressure capacity for precise low-temperature measurements with a large sample volume. Edited by: A. Goñi, A. Cantarero, J. S. Reparaz