A5075822605- Electrochemical sensors and biosensors
- Electrochemical Analysis and Applications
- Supercapacitor Materials and Fabrication
- Analytical Methods in Pharmaceuticals
- Advanced battery technologies research
- Catalytic C–H Functionalization Methods
- Electrocatalysts for Energy Conversion
- Conducting polymers and applications
- Analytical Chemistry and Sensors
- Nanomaterials for catalytic reactions
- Chemical Synthesis and Analysis
- Advanced Nanomaterials in Catalysis
- Advanced Photocatalysis Techniques
- Transition Metal Oxide Nanomaterials
- Pharmacological Effects and Assays
- ZnO doping and properties
- TiO2 Photocatalysis and Solar Cells
- Click Chemistry and Applications
- Pharmacology and Obesity Treatment
- Radical Photochemical Reactions
- Wound Healing and Treatments
- Dielectric materials and actuators
- Drug Solubulity and Delivery Systems
- Advanced Sensor and Energy Harvesting Materials
- Polyoxometalates: Synthesis and Applications
Indian Institute of Technology Jodhpur
2024
Yunnan University
2019
Sri Venkateswara University
2014-2018
Wuhan University of Science and Technology
2016-2018
Indian Institute of Technology Tirupati
2015
Jawaharlal Nehru Technological University, Hyderabad
2005
Reverse phase High performance liquid chromatography method has developed and validated for the simultaneous analysis of glibenclamide, metformin hydrochloride pioglitazone in tablet dosage form.The chromatographic separation drugs was achieved at ambient temperature with isocratic mode by using C 18 Hypersil BDS (150 x 4.6 mm, 5 µm) column mobile containing acetonitrile: 0.1M potassium dihydrogen orthophosphate buffer (pH 4.5 adjusted 10% sodium hydroxide solution) ratio 55: 45 v/v flow...
A novel an electrochemical sensor is constructed based on three-dimensional Nickel oxide nano flowers (3D-NiO) and TiO2-nanowire arrays (TiO2NWA) by hydrothermal route. Initially TiO2-NWA were produced titanium foil using method in the presence of 1.0 M NaOH solution at 180 °C for 20 h, then 3D-nickel (NiO) (up to 3 µM) are directly grown TiO2 NWA reaction glucose, urea nickel acetate mixer 150 5 followed N2 gas assisted annealing 500 2 h. The resultant nanostructures characterized CV, XRD,...
Pt as a chemical inert metal has been widely applied the counter electrode in various electrochemical measurements. However, it can also be dissolved and redeposit to working under certain circumstances. Herein we demonstrated cyclic voltammetry (CV) cycling method synthesize catalyst comprising inserted nanoparticles into MoS₂ nanoflake stack structures on stainless steel mesh (SSM). The binder-free composite structure exhibits significantly enhanced hydrogen evolution reaction (HER)...
Precious non-noble metals have been constantly attracting research attention in order to realize an inexpensive, extra active and more stable electrocatalysts terms of various oxidation states structures for their applications (splitting) water. In the present work graphene oxide incorporated, MnO2-NiO composite metal nanoflakes were synthesized on stainless steel substrate using efficient electrodeposition route alkaline media drop casting method with further annealing treatment at 400 °C 4...
The main objective of the current discussion was to decorate polypyrrole (PPy) supported with copper (Cu) nanoparticles on alkali anodized steel (AS) electrode for detection glucose in human saliva and serum samples. Initially, 10 M NaOH, then, electrodeposition method applied fabrication CuNPs PPy at room temperature. First time, we prepared this sensor by simple alkaline method. as-prepared represented as PPy/Cu/AS used an electrochemical sensor. As usual cyclic voltammetry, EIS, FESEM,...
There is a scarcity of general strategies for the site-selective α–Csp3–H arylation glycine derivatives to synthesize nonproteinogenic α-arylglycines that occur frequently in commercial drugs and bioactive molecules. We disclose copper-photoredox-catalyzed using diaryliodonium reagents (DAIRs) as arylating agents. This strategy harnesses underexplored ability DAIRs serve agents under visible-light irradiation copper salts photocatalysts. The method applies glycine-selective C–H peptides with...
Eh–pH diagrams of a Ca-S-H2O system at different conditions were described with thermodynamic calculations to investigate the leaching sulphur from desulphurisation slag. The influences temperature, oxygen partial pressure and activity dissolved species on hydrothermal systematically studied. results show that reactions occur spontaneously under normal leaches into leachate as S2−, HS−, H2S(aq), S(s) SO42−. At higher temperatures, HS− converts S2− or H2S(aq). Additionally, oxidise elemental...
An electrochemical sensor based on a palladium (Pd) and graphene (Gr) composite modified GCE was fabricated, characterised used for the simultaneous determination of OMT DCV in grain samples.
There is a scarcity of general strategies for the site-selective α-Csp3-H arylation glycine derivatives to synthesize non-proteinogenic α-arylglycines that occur frequently in commercial drugs and bioactive molecules. We disclose copper-photoredox catalyzed using diaryliodonium reagents (DAIRs) as aryl transfer agents. This strategy harnesses underexplored ability copper catalysts generate radicals from DAIRs under sustainable conditions. The method applies glycine-selective C-H peptides...
The electrochemical behaviour of Pioglitazone (PGZ) drug was studied using carbon paste electrode (CPE) in Britton Robinson (BR) buffer solution. Here Cyclic voltammetry and differential pulse voltammetric techniques were employed for this determination. reduction process shown to be irreversible over the pH range (2.0–10.0) well-defined peaks are obtained at -1.80V based on diffusion controlled. Effects cathodic peak potential, current ( I pa ), scan rate, pH, etc., have been discussed. A...
The primary goal of this research work was to develop a simple, precise, accurate and specific method for the estimation Ezetimibe Fenofibrate in bulk pharmaceutical dosage form by RP-HPLC.Method development carried out HPLC autosampler Schimadzu 2030C 3D Plus with stationary phase YMC C 8 column(150mmx 4.6mm.ld,3µ,12nm)using mobile Acetonitrile: Methanol: Phosphate buffer adjusted pH 3 OPA ratio 55:15:30v/v/v at flow rate 1.0mL/min injection volume 20µL detection is 255nm.The retention time...