A5033113575- Advancements in Battery Materials
- Advanced Battery Materials and Technologies
- Advanced NMR Techniques and Applications
- Advanced X-ray Imaging Techniques
- Metalloenzymes and iron-sulfur proteins
- X-ray Diffraction in Crystallography
- Organometallic Complex Synthesis and Catalysis
- Synthesis and characterization of novel inorganic/organometallic compounds
- Crystallization and Solubility Studies
- Advanced Electron Microscopy Techniques and Applications
- Advanced X-ray and CT Imaging
University of Illinois Urbana-Champaign
2010-2023
University of Regensburg
2023
Abstract The reaction between the heteroleptic metal carbonyl complex [W(CO) 4 (tmeda)] ((tmeda)= N , ′, ′‐Tetramethylethane‐1,2‐diamine) with [Si 9 ] 4− silicon Zintl clusters in presence of [2.2.2]crypt ([2.2.2]crypt=4,7,13,16,21,24‐Hexaoxa‐1,10‐diazabicyclo[8.8.8]‐hexacosane) liquid ammonia yielded compound [(K,Rb)@([2.2.2]crypt)] 2 (K,Rb) W(CO) ⋅ 13.4 NH 3 . was analyzed by single crystal X‐ray diffraction and crystallizes space group ( a =11.48390(10) Å, b =19.7383(2) c =19.8983(2) α...
High resolution x-ray computed tomography is a powerful non-destructive 3-D imaging method. It can offer superior on objects that are opaque or low contrast for optical microscopy. Synchrotron based systems have been available scientific research, but remain difficult to access broader users. This work introduces lab-based high-resolution nanotomography system with 50nm in absorption and Zernike phase modes. Using this system, we demonstrated high quality images of polymerized photonic...
Inorganic solid-state battery electrolytes show high ionic conductivities and enable the fabrication of all batteries. In this work, we present temperature dependence spin-lattice relaxation time (T1), spin-spin (T2), resonance linewidth () 7Li nuclear magnetic (NMR) for four (Li3InCl6 (LIC), Li3YCl6 (LYC), Li1.48Al0.48Ge1.52(PO4)3 (LAGP) LiPS5Cl (LPSC) from 173 K to 403 at a frequency 233 MHz, 253 353 291 MHz. Additionally, measured rates an effective 133 kHz using spin-locking pulse...
Inorganic solid-state battery electrolytes show high ionic conductivities and enable the fabrication of all batteries. In this work, we present temperature dependence spin-lattice relaxation time (T1), spin-spin (T2), resonance linewidth () 7Li nuclear magnetic (NMR) for four (Li3InCl6 (LIC), Li3YCl6 (LYC), Li1.48Al0.48Ge1.52(PO4)3 (LAGP) LiPS5Cl (LPSC) from 173 K to 403 at a frequency 233 MHz, 253 353 291 MHz. Additionally, measured rates an effective 133 kHz using spin-locking pulse...